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Tuesday, April 28, 2020 | History

2 edition of High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk found in the catalog.

High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk

Komoroski

High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk

  • 130 Want to read
  • 14 Currently reading

Published by John Wiley & Sons Inc .
Written in English

    Subjects:
  • Chemistry

  • The Physical Object
    FormatHardcover
    Number of Pages380
    ID Numbers
    Open LibraryOL10303746M
    ISBN 100471186708
    ISBN 109780471186700

    Carbon (C13) nuclear magnetic resonance (most commonly known as carbon NMR or 13 C NMR or sometimes simply referred to as carbon NMR) is the application of nuclear magnetic resonance (NMR) spectroscopy to is analogous to proton NMR (1 H NMR) and allows the identification of carbon atoms in an organic molecule just as proton NMR identifies hydrogen atoms.


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High-Resolution Nmr Spectroscopy of Synthetic Polymers in Bulk by Komoroski Download PDF EPUB FB2

This book is an authoritative and comprehensive account of the principles and practice of modern NMR spectroscopy of solid polymers to determine their structure and dynamics at a molecular level.

Book Review: High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk. Edited by R. KomoroskiAuthor: Hans Wolfgang Spiess. The various techniques used to analyze the microstructures of polymers are presented in this book.

High resolution and solid state techniques are described, and applications to both synthetic and biological polymers are discussed in detail. Particular emphasis is placed on the determination of polymer microstructure by NMR by: Book Review: High resolution NMR spectroscopy of synthetic polymers in bulk.

edited by Richard A. Komoroski, VCH Publishers, Deerfield Beach, FL,pp.price DM A practical guide to the study and understanding of the structure of synthetic polymer materials using the complete range of microscopic techniques.

The major part of the book is devoted to specimen preparation and applications. New applications and additional references provide a critical update. Category: Technology & Engineering.

About this book. This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers. It represents a deliberate attempt to pull together the numerous strands of the subject in a single comprehensive volume, designed to be readable at every scientific level.

This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

This book is a valuable resource for chemists and research workers. High Resolution NMR of Macromolecules presents the development in the NMR study of polymers. This book discusses the exciting area of application of NMR to polymer science as the result of the more general accessibility of instruments of high magnetic field.

Vulcanized rubbers, i.e., vulcanized natural rubber and vulcanized chloroprene rubber, were characterized by rubber-state NMR resolution 1 H and 13 C-NMR spectra were accomplished for the vulcanized rubbers due to fast magic angle spinning. The correlation between 1 H and 13 C of the vulcanized rubbers was investigated by one- and two-dimensional : Seiichi Kawahara, Yoshimasa Yamamoto, Takayuki Saito.

Abstract. High resolution nuclear magnetic resonance (HR-NMR) spectroscopy is the apellative given to the measurement of NMR spectra under conditions that enable magnetically nonequivalent nuclei of the same spin species (e.g., protons or carbon) to be resolved as individual resonance by: Description.

High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences.

It is written at an "intermediate". Description High Resolution NMR of Macromolecules presents the development in the NMR study of polymers. This book discusses the exciting area of application of NMR to polymer science as the result of the more general accessibility of instruments of high magnetic Edition: 1.

Reviews the principles and application of high resolution NMR in polymers. Triplet Exciton Generation in Bulk-Heterojunction Solar Cells Based on Endohedral Fullerenes.

Polymer Molecular Weight Analysis by 1H NMR Spectroscopy. Journal of Chemical Education88 (8), DOI: /edv. Cited by: 5. "NMR Spectroscopy of Polymers covers in detail all aspects of the NMR spectroscopic analysis of polymers.

this is an excellent reference book for synthetic polymer chemists and contains many useful practical points in addition to providing detailed coverage of the theoretical aspects of NMR spectroscopy.". Overview of NMR of Bulk Polymers Hans Wolfgang Spiess Chapter 2, DOI: /bkch Publication Date (Web): Octo Komoroski RA (ed) () High resolution NMR spectroscopy of Synthetic Polymers in Bulk.

VCH, New York Google Scholar Wind RA, Dec SF, Lock H, Maciel GE () J. Cited by: 1. Natural and Synthetic High Polymers: Lectures Presented at the Seventh Colloquium on N.M.R. Spectroscopy (NMR Basic Principles and Progress (4)) [Kosfeld, R.] on *FREE* shipping on qualifying offers.

Natural and Synthetic High Polymers: Lectures Presented at the Seventh Colloquium on N.M.R. Spectroscopy (NMR Basic Principles and Progress (4))Format: Paperback.

Experimental practice in high-resolution solution-state NMR of polymers 16 The spectrometer 16 The sample 17 Advanced Fourier transform techniques 18 One-dimensional techniques 19 Two-dimensional NMR spectroscopy 22 A survey of applications of high-resolution solution-state NMR to polymers trends in analytical chemistry, aol.

2, no. 3, Proton and carbon high resolution NMR spectroscopy of high polymers Using a super-conducting magnet, the examination of high polymers by 1H- and 13C-NMR provides complementary and precise information about their by: 3. Proton and Carbon NMR Spectra of Polymers.

Quang Tho Pham. Taylor & Francis, - Carbon - pages. 1 Review. Contains NMR spectra with associated analytical notes covering acrylics, 4/5(1). ISBN: OCLC Number: Description: xi, pages: illustrations ; 25 cm.

Contents: Overview of High-Resolution NMR of Solid Polymers; Principles and General Aspects of High-Resolution NMR of Bulk Polymers; High-Resolution NMR of Glassy Amorphous Polymers; Carbon NMR of Solid Amorphous Polymers Above Tg; Carbon Solid-State NMR.

“NMR Spectroscopy of Polymers” Tutorial. ACS National Meeting. New Orleans, April 6, Overview of NMR of Bulk Polymers.

Overview of NMR of Bulk Polymers. Proton NMR spectroscopy of solids has traditionally been challenging due to the widespread presence of strong ¹H-¹H dipolar couplings in solid systems, which severely broaden proton NMR spectral.

A Magnetic Resonance: Polymer Applications of NMR (NMR). Complexity in synthetic polymers arises for different reasons, which shall be The acquisition of high-resolution solid-state 19F spectra is a particular challenge because of its % abundance and high Larmor fre-File Size: KB.

Concentration: For 1H spectra (high resolution Δ1/2. Text Books: Understanding NMR Spectroscopy, James Keeler, John Wiley & Sons. ISBN High Resolution NMR Techniques in Organic Chemistry (Second Edition), T.D.W.

Claridge, Tetrahedron Organic Chemistry, Vol Elsevier. ISBNFile Size: 1MB. Where a substance in the solid state is concerned, high‐resolution 13 C‐NMR spectroscopy provides not only information about the chemical structure, but also about the solid state itself.

To mention just a few examples, information on the conformation, crystal structure and molecular dynamics, as well as molecular miscibility is given. Polymer Applications of Solid-State NMR Polymers Above T g: Elastomers and Melts High-resolution MAS MQ NMR on elastomers and melts Polymers Around and Below T g Conformations of polymers in the glassy state   Nuclear magnetic resonance (NMR) spectroscopy is a premiere technique for the studies of polymers.

It is widely used for polymer identification, quality control, and reaction monitoring to structure determination, polymer morphology, compatibility, chain. High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk by R. Komoroski A copy that has been read, but remains in clean condition.

All pages are intact, and the cover is intact. The spine may show signs of wear. Pages can include limited notes and highlighting, and the copy can include previous owner inscriptions. • Can use 13C-NMR to detect and quantify these different types of branching • This technique is based upon the chemical shifts of the carbon atoms on the backbone chain attached to the branch.

• The chemical shift depends on the length of the branch for branches up to 6 carbons in length. It is the same for all branches 6 carbons and longer. Download books "Physics - Spectroscopy". Ebook library | B–OK. Download books for free.

Find books NMR Spectra of Polymers and Polymer Additives A J Brandolini D D Hills Marcel Dekker 0. CRC Press. High-Resolution NMR Techniques in Organic Chemistry (Tetrahedron Organic Chemistry) T. Claridge. Year. This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers.

It represents a deliberate attempt to pull together the numerous strands of the subject in a single comprehensive volume, designed to be readable at every scientific level.

It is Price: $ high resolution nmr spectra This page describes how you interpret simple high resolution nuclear magnetic resonance (NMR) spectra. It assumes that you have already read the background page on NMR so that you understand what an NMR spectrum looks like and the use of the term "chemical shift".

Brandolini and C. Dybowski, "High-Resolution NMR of Oriented Polymers", in High-Resolution NMR Spectroscopy of Synthetic Polymers in Bulk (ed. Komoroski). This book provides a source of information on all major aspects of NMR spectroscopy of synthetic polymers.

Readers new to NMR will find extensive information within the book on the available techniques, allowing full exploration of the many polymer science applications. Theory. The chemical theory that underlies NMR spectroscopy depends on the intrinsic spin of the nucleus involved, described by the quantum number S.

Nuclei with a non-zero spin are always associated with a non-zero magnetic moment, as described by Equation \ref{1}, where μ is the magnetic moment, \(S\) is the spin, and γ is always non-zero. Solid-state NMR spectroscopy insoluble compounds (synthetic polymers) very large compounds (requires specific labels) determination of the structure in the solid-state (vs.

liquid-state) determination of the dynamics in the solid-state Imaging techniques spin tomography "In vivo" NMR spectroscopy distribution of metabolites in the body. acterization of the polymers under study by nuclear magnetic resonance (NMR) spectroscopy.

In addition to monitoring the various synthetic steps, which eventually lead to the new polymers or supramolecular systems des-cribed, high-resolution NMR provides a number of impor-tant parameters, which are specific to macromolecules.[1] Examples are Cited by: 8.

In the second part, applications of NMR to a variety of polymer systems in the solid state are es of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book.

Proton and Carbon NMR Spectra of Polymers is an updated, consolidated volume featuring the spectra published in three previous volumes, plus newly derived spectra. It contains NMR spectra with associated analytical notes covering acrylics, amides, dienes, ethers, olefins, siloxins, styrene.6) R.

A. Komoroski, “High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk”, VCH, New York 7) J. V. McBrierty, K. J. Packer, “Nuclear Magnetic Resonance in Solid Polymers”, Cambridge University Press, New York 8) K.

Schmidt-Rohr, H. W. Spiess, “Multidimen sional Solid-State NMR and Polymers”, Academic Press.spinning frequency resolution of NMR spectra significantly improves. However, in the case of a dense network of strongly dipolar-coupled spins like 1H the line-widths of NMR signals are frequency dependent and all signals are still broad.

Even at moderately fast spinning speeds 1H NMR spectra remain featureless. Sufficient resolution is provided by.